{"id":130,"date":"2017-06-12T14:12:55","date_gmt":"2017-06-12T18:12:55","guid":{"rendered":"https:\/\/carleton.ca\/manthorpe\/?page_id=130"},"modified":"2025-03-05T19:40:20","modified_gmt":"2025-03-06T00:40:20","slug":"publications","status":"publish","type":"page","link":"https:\/\/carleton.ca\/manthorpe\/publications\/","title":{"rendered":"Publications"},"content":{"rendered":"

Publications from Independent Career:<\/strong><\/em><\/span><\/h3>\n

36. Benjamin B. Warnes, Jasmine Chihabi, Jeffrey M. Manthorpe*
\n<\/strong>“Unveiling Readily Ionized and Robust Anionic Species: A Gateway to Enhanced Ionization Efficiency in ESI-MS Analysis”
\nJournal of the American Society for Mass Spectrometry<\/em>, 2025<\/strong>, 36<\/em>, 524-533. Journal Link<\/a> or ChemRxiv Link (free\/open source preprint)<\/a><\/p>\n

35. Christian A. Rosales, Noah A. Lepinsky, Wondewassen Gebeyehu, Karl V. Wasslen, Fraser Colquhoun, Benjamin B. Warnes, Jasmine Chihabi, Jeffrey M. Manthorpe*, Jeffrey C. Smith*
\n<\/strong>“Improved LC-MS Detection of Opioids, Amphetamines, and Psychedelics Using TrEnDi”
\nJournal of the American Society for Mass Spectrometry<\/em>, 2025<\/strong>, 36<\/em>, 514-523. Journal Link<\/a> or ChemRxiv Link (free\/open source preprint)<\/a><\/p>\n

34. Volodymyr Semeniuchenko, Sepideh Sharif, Neha Rana, Nalin Chandrasoma, Wilfried M. Braje, R. Tom Baker, Jeffrey M. Manthorpe, William J. Pietro, Michael G. Organ*
\n<\/strong>“Experimental Evidence for Zerovalent Pd(NHC) as a Competent Catalyst in C\u2013N Cross-Coupling (NHC = DiMeIHept^Cl)
\nJournal of the American Chemical Society,<\/em> 2024<\/strong>, 146<\/em>, 29224-29236. Journal Link<\/a><\/p>\n

33. Joshua A. Roberts, Angela S. Radnoff, Aleksandra Bushueva, Jocelyn A. Menard, Karl V. Wasslen, Meaghan Harley, Jeffrey M. Manthorpe*, Jeffrey C. Smith*
\n<\/strong>“Mobile Phase Contaminants Affect Neutral Lipid Analysis in LC-MS-based Lipidomics Studies”
\nJournal of the American Society for Mass Spectrometry<\/em>, 2024<\/strong>, 35<\/em>, 3095-3106. Journal Link<\/a> or ChemRxiv Link (free\/open source preprint)<\/a><\/p>\n

32. Samuel W. J. Shields, Carlos R. Canez, Christian A. Rosales, Joshua A. Roberts, Hilary Bourgaize, Peter J. Pallister, Jeffrey M. Manthorpe*, Jeffrey C. Smith*
\n<\/strong>“Optimized 13C-TrEnDi Enhances the Sensitivity of Plasmenyl Ether Glycerophospholipids and Demonstrates Compatibility with Other Derivatization Strategies”
\nJournal of the American Society for Mass Spectrometry<\/em>, 2024<\/strong>, 35<\/em>, 972-981. Journal Link<\/a> or ChemRxiv Link (free\/open source preprint)<\/a><\/p>\n

31. Christian A. Rosales, Krysten L. Sheedy, Karl V. Wasslen, Jeffrey M. Manthorpe*, Jeffrey C. Smith*
\n<\/strong>“Trimethylation Enhancement Using Diazomethane (TrEnDi) Enables Enhanced Detection of Glufosinate and 3-(Methylphosphinico)propionic Acid from Complex Canola Samples”
\nJournal of the American Society for Mass Spectrometry<\/em>, 2024<\/strong>, 35<\/em>, 140-150. Journal Link<\/a> or ChemRxiv Link (free\/open source preprint)<\/a><\/p>\n

30. Joshua A. Roberts, Christian A. Rosales, Karl V. Wasslen, Angela S. Radnoff, Elena Godbout, Jean-Simon Diallo, Jeffrey M. Manthorpe*, Jeffrey C. Smith*
\n<\/strong>“An In Silico Database for Automated Feature Identification of High-Resolution Tandem Mass Spectrometry 13<\/sup>C Trimethylation Enhancement Using Diazomethane (13<\/sup>C-TrEnDi)-Modified Lipid Data”
\nJournal of the American Society for Mass Spectrometry<\/em>, 2023<\/strong>, 34<\/em>, 2722-2730. Journal Link<\/a> or ChemRxiv Link (free\/open source preprint)<\/a><\/p>\n

29. Christian A. Rosales, Samuel W. J. Shields, Chelsey Aulenback, Elezi Gazmend, Karl V. Wasslen, Peter Pallister, Kym Faull, Jeffrey M. Manthorpe*, Jeffrey C. Smith*
\n<\/strong>“Improved chromatography and MS-based detection of glyphosate and aminomethylphosphonic acid using iTrEnDi”
\nJournal of the American Society for Mass Spectrometry<\/em>, 2023<\/strong>, 34<\/em>, 948-957. Journal Link<\/a><\/p>\n

28. Volodymyr Semeniuchenko, Sepideh Sharif, Jonathan Day, Nalin Chandrasoma, William J. Pietro, Jeffrey M. Manthorpe, Wilfried M. Braje, Michael G. Organ*
\n<\/strong>“(DiMeIHeptCl)Pd: A Low-Load Catalyst for Solvent-Free (Melt) Amination”
\nJournal of Organic Chemistry<\/em>, 2021<\/strong>, 86<\/em>, 10343-10359. LINK<\/a><\/p>\n

27. Mathieu A. Morin, Debasis Mallik, Wenyao Zhang, William Pietro, Jeffrey M. Manthorpe, Michael G. Organ*
\n<\/strong>\u201cObtaining Kinetics from Continuous Processes: Sampling Multiple Time Point Concurrently With a Single Valve Rotation
\nChemistry\u2014Methods <\/em>(Open Access), 2021<\/strong>, 1<\/em>, 131. LINK<\/a><\/p>\n

26. Monica A. Gill, Samuel W. J. Shields, Jeffrey M. Manthorpe*
\n<\/strong>\u201cOrigin of Protonation Side Products in Pd-Catalyzed Decarboxylative Allylation Reactions: Evidence for In Situ Modification of Triphenylphosphine Ligand\u201d
\nChemRxiv<\/em>, Feb 2021<\/strong> LINK<\/a><\/p>\n

25. Samuel W. J. Shields, Christian A. Rosales, Joshua A. Roberts, Peter Pallister, Karl V. Wasslen, Jeffrey M. Manthorpe*, and Jeffrey C. Smith*
\n<\/strong>\u201ciTrEnDi: In Situ Trimethylation Enhancement Using Diazomethane: Improved and Expanded Glycerophospholipid and Sphingolipid Analyses via a Microscale Autonomous Derivatization Platform\u201d
\nAnalytical Chemistry<\/em>, 2021<\/strong>, 93<\/em>, 1084-1091. LINK<\/a><\/p>\n

24. Elissia T. Franklin, Samuel W. J. Shields, Jeffrey M. Manthorpe, Jeffrey C. Smith, Yu Xia, and Scott A. McLuckey*
\n<\/strong>\u201cCoupling Headgroup and Alkene Specific Solution Modifications with Gas-Phase Ion\/Ion Reactions for Sensitive Glycerophospholipid Identification and Characterization\u201d
\nJournal of the American Society for Mass Spectrometry<\/em>, 2020<\/strong>, 31<\/em>, 938-945. LINK<\/a><\/p>\n

23. Monica A. Gill and Jeffrey M. Manthorpe
\n<\/strong>\u201cDevelopment of Palladium-Catalyzed Decarboxylative Allylation of Electron-Deficient Sulfones and Identification of Unusual Side Products\u201d
\nJournal of Organic Chemistry<\/em>, 2019<\/strong>, 84<\/em>, 6028-6039. LINK<\/a><\/p>\n

22. <\/span><\/strong>Samuel W. J. Shields, Peter H. Buist, and Jeffrey M. Manthorpe*
\n<\/strong><\/span>\u201cAsymmetric and Regiospecific Synthesis of Isotopically Labelled Cyclopropane Fatty Acid (9<\/span>R<\/span><\/em>,10<\/span>S<\/span><\/em>)-Dihydrosterculic Acid: Overcoming Spontaneous Protonation During Lithium-Sulfoxide Exchange\u201d
\n<\/span>SynOpen<\/em> (Open Access),\u00a02018<\/strong>, 2<\/em>, 168-175. LINK<\/a><\/span><\/p>\n

21. Stella K. Betancourt,\u00a0Carlos R. Canez, Samuel W. J. Shields, Jeffrey M. Manthorpe, Jeffrey C. Smith, and Scott A. McLuckey*
\n<\/span><\/strong>“Trimethylation Enhancement using <\/span>13<\/span>C-Diazomethane (<\/span>13<\/span>C-TrEnDi): Gas-Phase Charge Inversion of Modified Phospholipid Cations for Enhanced Structural Characterization”
\n<\/span>Analytical Chemistry <\/span><\/em>2017<\/span><\/strong>, <\/span>89<\/span><\/em>, 9452-9458. LINK<\/a><\/span><\/p>\n

20.<\/span><\/strong> Carlos R. Canez, Samuel W. J. Shields, Magdalena Bugno, Karl V. Wasseln, Hillary P. Weinert, William G. Willmore, Jeffrey M. Manthorpe*, and Jeffrey C. Smith*
\n<\/strong><\/span>\u201cTrimethylation Enhancement using <\/span>13<\/span>C-Diazomethane (<\/span>13<\/span>C-TrEnDi): Increased Sensitivity and Selectivity of Phosphatidylethanolamine, Phosphatidylcholine and Phosphatidylserine Lipids Derived from Complex Biological Samples\u201d
\n<\/span>Analytical Chemistry <\/span><\/em>2016<\/span><\/strong>, <\/span>88<\/span><\/em>, 6996-7004<\/span>. <\/span>LINK<\/a>
\n<\/span><\/p>\n

19. <\/span><\/strong>Noof A. Alenazi, Jeffrey M. Manthorpe, Edward P. C. Lai*
\n<\/strong><\/span>\u201cSelectivity Enhancement in Molecularly Imprinted Polymers for Chemical Sensing of Bisphenol A\u201d
\nSensors<\/em>\u00a0(Open Access)\u00a02016<\/span><\/strong>, <\/span>16<\/em>, 1697 (12 pages).<\/span> (Invited contribution to thematic issue on Molecular Imprinting for Transducers and Applications). LINK<\/a>
\n<\/span><\/p>\n

18. <\/span><\/strong>Noof A. Alenazi, Jeffrey M. Manthorpe, and Edward P. C. Lai*
\n<\/strong><\/span>\u201cSelective Extraction of BPA in Milk Analysis by Capillary Electrophoresis using a Chemically Modified Molecularly Imprinted Polymer\u201d
\nFood Control<\/em> 2015<\/span><\/strong>, <\/span>50<\/em>, 778-783. <\/span>LINK<\/a>
\n<\/span><\/p>\n

17.<\/span><\/strong> Karl V. Wasslen, Carlos R. Canez, Hyunmin Lee, Jeffrey M. Manthorpe*, and Jeffrey C. Smith*
\n<\/strong><\/span>\u201cTrimethylation Enhancement using Diazomethane (TrEnDi) II: Rapid In-Solution Concomitant Quaternization of Glycerophospholipid Amino Groups and Methylation of Phosphate Groups via Reaction with Diazomethane Significantly Enhances Sensitivity in Mass Spectrometry Analyses via a Fixed, Permanent Positive Charge\u201d
\n<\/span>Analytical Chemistry <\/span><\/em>2014<\/span><\/strong>, <\/span>86<\/span><\/em>, 9523-9532.<\/span> LINK<\/a>
\n<\/span><\/p>\n

16. <\/span><\/strong>Samuel W. J. Shields and Jeffrey M. Manthorpe*
\n<\/strong><\/span>\u201cEfficient, Scalable, and Economical Preparation of tris(Deuterium)- and <\/span>13<\/span>C-Labelled <\/span>N<\/span><\/em>-Methyl-<\/span>N<\/span><\/em>-Nitroso-<\/span>p<\/span><\/em>-Toluenesulfonamide (Diazald\u00ae) and their Conversion to Labelled Diazomethane\u201d
\n<\/span>Journal of Labelled Compounds and Radiopharmaceuticals<\/span><\/em> 2014<\/span><\/strong>, <\/span>57<\/span><\/em>, 674-679.<\/span> LINK<\/a>
\n<\/span><\/p>\n

15. <\/span><\/strong>Noof A. Alenazi, Edward P. C. Lai, and Jeffrey M. Manthorpe*
\n<\/strong><\/span>\u201cEnhanced Selectivity of a Molecularly Imprinted Polymer toward the Target Molecule via Esterification of Non-Specific Binding Sites with Diazomethane\u201d
\nJournal of Molecular Recognition<\/em> 2014<\/span><\/strong>, <\/span>27<\/em>, 755-762. <\/span>LINK<\/a>
\n<\/span><\/p>\n

14. <\/span><\/strong>Karl V. Wasslen, Le Hoa Tan, Jeffrey M. Manthorpe*, and Jeffrey C. Smith*
\n<\/strong><\/span>\u201cTrimethylation Enhancement using Diazomethane (TrEnDi): Rapid On-Column Quaternization of Peptide Amino Groups via Reaction with Diazomethane Significantly Enhances Sensitivity in Mass Spectrometry Analyses via a Fixed, Permanent Positive Charge\u201d
\n<\/span>Analytical Chemistry <\/span><\/em>2014<\/span><\/strong>, <\/span>86<\/span><\/em>, 3291-3299<\/span>. <\/span>LINK<\/a>
\n<\/span><\/p>\n

13. <\/span><\/strong>Jeffrey M. Manthorpe*, Han Il Kong, John W. Palko, and Monica A. Gill
\n<\/strong><\/span>\u201cReduction of Sulfur\u2013Carbon Bonds and of Other Heteroatoms Bonded to Tetrahedral Carbon\u201d
\nComprehensive Organic Synthesis, 2nd Edition<\/em>;<\/span> Molander, G. A., Knochel, P., Eds; Elsevier: Oxford, 2014<\/strong>; Vol. 8<\/em>, pp 1031-1085. <\/span>LINK<\/a>
\n<\/span><\/p>\n

12.<\/span><\/strong> John W. Palko, Peter H. Buist, and Jeffrey M. Manthorpe*
\n<\/strong><\/span>\u201cA Flexible and Modular Stereoselective Synthesis of (9<\/span>R<\/span><\/em>,10<\/span>S<\/span><\/em>)-Dihydrosterculic Acid\u201d
\n<\/span>Tetrahedron: Asymmetry<\/span><\/em> 2013<\/span><\/strong>, <\/span>24<\/span><\/em>, 165-168. <\/span>LINK<\/a>
\n<\/span><\/p>\n

11.<\/span><\/strong> Han Il Kong, Monica A. Gill, Amy H. Hrdina, Jennifer E. Crichton, and Jeffrey M. Manthorpe*
\n<\/strong><\/span>\u201cReactivity of <\/span>\u03b1<\/span>-Trifluoromethanesulfonyl Esters, Amides and Ketones: Decarboxylative Allylation, Methylation, and Enol Formation\u201d
\n<\/span>Journal of Fluorine Chemistry<\/span><\/em>, <\/span>2013<\/span><\/strong>, <\/span>153<\/span><\/em>, 151-168<\/span>. <\/span>LINK<\/a>
\n<\/span><\/p>\n

10.<\/span><\/strong> Monica A. Gill and Jeffrey M. Manthorpe*
\n<\/strong><\/span>\u201cMild, Rapid, and Inexpensive Microwave-Assisted Synthesis of Allylic and Propargylic Esters\u201d
\n<\/span>Synthetic Communications <\/span><\/em>2013<\/span><\/strong>, <\/span>43<\/span><\/em>, 1460-1468<\/span>. <\/span>LINK<\/a>
\n<\/span><\/p>\n

9.<\/span> Han Il Kong, Jennifer E. Crichton, and Jeffrey M. Manthorpe*
\n<\/strong>\u201cStereoselective Synthesis of Ambiphilic Alkenes via Regioselective Methylation of \u03b1<\/span>-Trifluoromethansulfonyl Carbonyl Compounds with Trimethylsilyldiazomethane\u201d
\nTetrahedron Letters<\/em> 2011<\/span><\/strong>, <\/span>52<\/em>, 3714-3717. <\/span>LINK<\/a><\/p>\n

<\/h3>\n

Publications from\u00a0<\/strong><\/em><\/span>Postdoctoral, Graduate and Undergraduate Studies<\/strong><\/em><\/span>:<\/strong><\/em><\/span><\/h3>\n

8.<\/span> Alex M. Szpilman, Damiano M. Cereghetti, Jeffrey M. Manthorpe, Nicholas R. Wurtz, and Erick M. Carreira
\n<\/strong>\u201cSynthesis and Biophysical Studies on 35-Deoxy Amphotericin B Methyl Ester\u201d
\nChemistry, A European Journal<\/em> 2009<\/span><\/strong>, <\/span>15<\/em>, 7117-7128. <\/span>LINK<\/a><\/p>\n

7. <\/span>Alex M. Szpilman, Jeffrey M. Manthorpe, and Erick M. Carreira
\n<\/strong>\u201cSynthesis and Biological Studies of 35-Deoxy Amphotericin B Methyl Ester\u201d
\nAngewandte Chemie International Edition<\/em> 2008<\/span><\/strong>, <\/span>47<\/em>,\u00a04339-4342<\/span>. <\/span>LINK<\/a>
\n<\/span><\/p>\n

6. <\/span>Alex M. Szpilman, Damiano M. Cereghetti, Nicholas R. Wurtz, Jeffrey M. Manthorpe, and Erick M. Carreira
\n<\/strong>\u201cSynthesis of 35-Deoxy Amphotericin B Methyl Ester: A Strategy for Molecular Editing\u201d
\nAngewandte Chemie International Edition<\/em> 2008<\/span><\/strong>, <\/span>47<\/em>, 4335-4338. <\/span>LINK<\/a>
\n<\/span><\/p>\n

5. <\/span>Az\u00e9lie Arpin, Jeffrey M. Manthorpe, and James L. Gleason
\n<\/strong>\u201cA Practical Chiral Bicyclic Thioglycolate Lactam Auxiliary for Stereoselective Quaternary Carbon Formation\u201d
\nOrganic Letters<\/em> 2006<\/span><\/strong>, <\/span>8<\/em>, 1359-1362. <\/span>LINK<\/a><\/p>\n

4. <\/span>Jeffrey M. Manthorpe, Alex M. Szpilman, and Erick M. Carreira
\n<\/strong>\u201cA Scalable Synthesis of a Mycosamine Donor. Overcoming Difficult Reactivity in Allose Systems\u201d
\nSynthesis <\/span><\/em>2005<\/span><\/strong>, 3380-3388. LINK<\/a><\/p>\n

3. <\/span>Jeffrey M. Manthorpe and James L. Gleason
\n<\/strong>“Asymmetric Synthesis of Quaternary Carbon Centers. Alkylation of \u03b1,\u03b1<\/span>-Disubstituted Enolates Generated by Reduction of Bicyclic Thioglycolate Lactams”
\nAngewandte Chemie International Edition<\/em> 2002<\/span><\/strong>, <\/span>41<\/em>, 2338-2341. LINK<\/a><\/span>
\n<\/span><\/p>\n

2.<\/span> Gordon L. Lange, Craig C. Humber, and Jeffrey M. Manthorpe
\n<\/strong>“[2+2] Photoadditions with Chiral 2,5-Cyclohexadienone Synthons”
\nTetrahedron: Asymmetry<\/em> 2002<\/span><\/strong>, <\/span>13<\/em>, 1355-1362. <\/span>LINK<\/a>
\n<\/span><\/p>\n

1. <\/span>Jeffrey M. Manthorpe and James L. Gleason
\n<\/strong>“Stereoselective Generation of E- and Z- Disubstituted Amide Enolates.\u00a0 Reductive Enolate Formation from Bicyclic Thioglycolate Lactams”
\nJournal of the American Chemical Society<\/em> 2001<\/span><\/strong>,<\/span> 123<\/em>, 2091-2092. <\/span>LINK<\/a>
\n<\/span><\/p>\n","protected":false},"excerpt":{"rendered":"

Publications from Independent Career: 36. Benjamin B. Warnes, Jasmine Chihabi, Jeffrey M. Manthorpe* “Unveiling Readily Ionized and Robust Anionic Species: A Gateway to Enhanced Ionization Efficiency in ESI-MS Analysis” Journal of the American Society for Mass Spectrometry, 2025, 36, 524-533. Journal Link or ChemRxiv Link (free\/open source preprint) 35. Christian A. Rosales, Noah A. Lepinsky, […]<\/p>\n","protected":false},"author":5,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"_relevanssi_hide_post":"","_relevanssi_hide_content":"","_relevanssi_pin_for_all":"","_relevanssi_pin_keywords":"","_relevanssi_unpin_keywords":"","_relevanssi_related_keywords":"","_relevanssi_related_include_ids":"","_relevanssi_related_exclude_ids":"","_relevanssi_related_no_append":"","_relevanssi_related_not_related":"","_relevanssi_related_posts":"","_relevanssi_noindex_reason":"","_mi_skip_tracking":false,"_exactmetrics_sitenote_active":false,"_exactmetrics_sitenote_note":"","_exactmetrics_sitenote_category":0,"footnotes":"","_links_to":"","_links_to_target":""},"yoast_head":"\nPublications - Manthorpe<\/title>\n<meta name=\"description\" content=\"Publications from Independent Career: 36. Benjamin B. Warnes, Jasmine Chihabi, Jeffrey M. 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